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41.
《Ceramics International》2022,48(17):24346-24354
The borided layer was prepared on the surface of the Ti–5Mo–5V–8Cr–3Al alloy by powder-pack boriding at 1000°C-10h. SEM, EPMA and TEM were used to investigate the effects of alloying elements (Al, V, Mo and Cr) on the growth of TiB whiskers in the borided Ti–5Mo–5V–8Cr–3Al alloy. Wear properties of borided Ti–5Mo–5V–8Cr–3Al alloy were investigated using dry reciprocating friction tests. SEM results show that the thickness of boride layer in Ti–5Mo–5V–8Cr–3Al alloy is thinner than that in the Cp-Ti. This is attributed to the enrichment of alloying elements especially V in TiB/substrate by TEM, which hinders the diffusion of B atoms, thus resulting in the short and thick TiB whiskers in Ti–5Mo–5V–8Cr–3Al alloy. Borided Ti–5Mo–5V–8Cr–3Al alloy has the better wear resistance than as-received alloy. 相似文献
42.
《Ceramics International》2022,48(3):3762-3770
Cf/Hf0.5Zr0.5C-SiC composites were prepared by introducing Hf0.5Zr0.5C matrix (11 cycles) and SiC matrix (9 cycles) into the carbon cloth preform through precursor impregnation and pyrolysis (PIP) process. The influence of the introduction time of SiC matrix on the microstructure and mechanical properties of Cf/Hf0.5Zr0.5C-SiC composites was studied, and the results show that with the increase of the PIP cycles of the SiC matrix introduced before Hf0.5Zr0.5C matrix, the composite open porosity decreased, and the flexural strength and modulus presented an obvious upward trend. CS45 sample, which has 4 cycles of PIP SiC introduced in advance, has the highest flexural strength, flexural modulus and interfacial shear strength of 402.73 ± 35.73 MPa, 56.92 ± 3.97 GPa and 100.88 ± 7.79 MPa, respectively. Hf0.5Zr0.5C matrix has a loose and porous structure, so when more SiC matrix was introduced in advance, its covering effect on the surface of fibers led to less intra-bundle pores and thusly denser composite structure, and due to the compactness of SiC matrix, better overall bonding of fiber, interface and matrix was achieved, as well as better load transfer effect, which led to obvious interfacial debonding and cracking based on the in-situ SEM observation during flexural tests. While in the sample without pre-introduced SiC, the cracking occurred mainly between the interface and porous matrix and the overall performance of the material was poor. 相似文献
43.
《Ceramics International》2022,48(6):8228-8234
This paper introduces a novel process to efficiently utilize medium-/low-grade or waste bauxite. The medium-/low-grade or waste bauxite is usually rich in iron oxide (total iron oxide content≥8%) or titanium dioxide (titanium dioxide content≥5%). In addition, both iron oxide and titanium dioxide have higher contents than typical bauxite (total iron oxide + titanium dioxide contents≥20%). It is difficult to obtain mullite with excellent properties using the process of beneficiation and sintering synthesis. Based on different reduction temperatures of K2O, Na2O, FeOx, SiO2 and TiO2, the reduction of K2O, Na2O and FeOx was set as the reduction end point. While SiO2 start to be reduced, TiO2 was unstable under high temperature and low oxygen partial pressure. The reason for the final formation of Ti2O3 in the TiO2→TiO2-x transformation process was analysed, and the morphology of the multiphase material obtained from the Ti2O3–3Al2O3·2SiO2 solid solution was characterized. The reaction model was established. 相似文献
44.
The structure and properties of Mn-doped 0.67BiFeO3-0.33BaTiO3 ceramics are systematically investigated with respect to the effects of annealing prior to rapid cooling by quenching in air. Air-quenching induces a change in crystal structure from pseudo-cubic to rhombohedral, with higher quenching temperatures leading to an increased rhombohedral distortion. These structural changes are correlated with the appearance of more well-defined ferroelectric domain configurations. It is shown that the surface preparation procedures for XRD measurements can induce significant changes in the peak profiles, indicating differences in crystal structure between the surface and bulk regions. Frequency dispersion in the temperature-dependent relative permittivity for the as-sintered sample is significantly reduced after quenching, accompanied by enhancement of the Curie point and improved temperature-stability of piezoelectric properties. It is proposed that the formation of defect clusters by A-site cation diffusion during cooling is circumvented by quenching, leading to the observed modification of structural distortion and ferroelectric properties. 相似文献
45.
《Ceramics International》2022,48(3):3536-3543
We investigated the optical and electrical properties of Ta2O5/Ag/Ta2O5 films as functions of the thicknesses of the Ta2O5 and Ag layers. It was found that with an increase in the thicknesses of the Ta2O5 and Ag layers from 10 to 40 nm and from 12 to 24 nm, respectively, the sheet resistance, carrier concentration, electron mobility, and resistivity of the Ta2O5/Ag/Ta2O5 film varied from 2.02 to 8.95 Ω/sq, 5.74 × 1021 to 2.92 × 1022 cm–3, from 13.21 to 24.07 cm2/V·s, and from 8.89 × 10-6 to 8.24 × 10-5 Ω cm, respectively. The average transmittance (Tav) of the multilayer samples ranged from 57.18% to 93.99%, and it depended on the Ta2O5 and Ag layer thicknesses. The highest Tav of 93.99% was observed for the film with 35 nm thick Ta2O5 and 18 nm thick Ag layers, and the peak Haacke's figure of merit (157.04 × 10–3 Ω–1) was obtained for 20 nm thick Ta2O5 and 21 nm thick Ag layers. Ta2O5 (100 nm) and Ta2O5/Ag/Ta2O5 (20 nm/21 nm/20 nm) samples had optical bandgaps of 4.70 and 4.45 eV, respectively. Film Wizard simulations were conducted to understand the dependence of the transmittance of the multilayer on the thicknesses of the Ta2O5 and Ag layers, and phasor analyses were performed to determine how the transmittance of the Ta2O5/Ag/Ta2O5 (20 nm/21 nm/20 nm) film depended on the Ta2O5 layer's thickness. 相似文献
46.
介绍了国家专利注锚剂、中空注浆锚索等产品,以国家能源麦朵山煤矿11采区2煤辅助运输巷为研究对象,采用数值模拟、理论分析、现场测试及井下试验相结合的综合研究方法,对11采区2煤辅助运输巷采用锚注一体联合支护技术,来实现对岩体裂隙注浆,使浆料与岩体结为一体,在围岩与支护体共同作用过程中,实现强岩增荷的作用,维护巷道的稳定性,实现工作面的安全生产。 相似文献
47.
《Ceramics International》2022,48(6):8025-8030
In order to meet the high demand for joining ceramic/superalloy composite structure in extreme environments, a novel high-temperature resistant adhesion technique was developed for joining ZrO2 and Inconel 625 by applying an aluminum phosphate emulsion/zirconium sol based adhesive. With increasing temperature, a series of reactions occurred in adhesive, and its high-temperature bonding was attributed to the formation of a composite structure containing various ceramics and intermetallics. The adhesive after RT curing could find direct applications in extreme environments, and provide bonding strength no less than 2.5 MPa in the temperature range of RT-1100 °C. The bonding strength was higher than 4 MPa in the temperature range of 800–1000 °C, which was further attributed to the formation of an effective CTE-gradient relationship among ZrO2, adhesive and Inconel 625, as well as the interfacial reactions between the two substrates. The work broadened the application of adhesion technique and brought new ideas for joining dissimilar engineering materials. 相似文献
48.
49.
《Ceramics International》2022,48(3):3600-3608
In the present study, the mechanical properties and microstructure of C/Mullite composites with a PyC-SiC double-layer interfacial coating after annealing were systematically studied to evaluate the evolution of thermal stability in an inert atmosphere and a vacuum. The C/Mullite composites annealed in the inert atmosphere exhibited better thermal stability than those annealed under the vacuum. The main factor for failure of the composites was carbothermal reduction. The activation temperature of carbothermal reduction in composites in the inert atmosphere was ~100 °C higher than that in the vacuum. Once carbothermal reduction was activated, the microstructure of composites was destroyed, resulting in a significant weight loss and mechanical property degeneration. The degeneration of mechanical properties was unrecoverable. 相似文献
50.
随着大数据时代的到来,智慧城市等一系列概念的提出,人工智能开始在城市各个角落得到广泛应用。其中,车牌识别作为城市道路交通重要的一环,也取得了重大突破。基于深度学习的车牌识别一经提出,各类算法应用于车牌检测及识别上,对比于传统的车牌识别,大大提高了识别的速率和准确率。然而,在非限制条件下,如大角度车牌识别准确率仍有提升的空间。提出了一种改进的FasterR-CNN与YOLO的深度学习车牌识别算法,将对大角度下的车牌识别准确率达到了99.7%。由于是轻量型的框架,为后续的移动设备部署工作提供了便利。 相似文献